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实验室反应釜的使用与保养及使用注意事项

时间:2017-10-25作者:舜甫科技 点击:
一、使用与保养
 
  使用实验室反应釜必须关闭冷媒进管阀门,放防病锅内和夹套内的剩余冷媒,再输入物料,开动搅拌器,然后开启蒸汽阀门和电热电源,到达所需温度后,应先关闭蒸汽阀门和电热电源,过2~3分钟后,再关搅拌器,加工结束后,放尽锅内和夹套剩余冷凝水后,应尽快用温水冲洗,刷掉粘糊着的物料,然后用40~500C碱水在容器内壁全面清洗,并用清水冲洗,特别锅内无物料(吸热介质)空锅情况下,不得开启蒸汽阀门和电热电源,特别注意使用蒸汽压力,不得超过定额工作压力。保养实验室反应釜要经常注意整台设备和减速器的工作情况,减速器润滑油不足应立即补充,电加热介质油每半年要进行更换,对夹套和锅盖上等部位的安全阀、压力表、温度表、蒸馏孔、电热棒、电器仪表等要应定期检查,如果有故障要即时调换或修理,设备不用时,一定用温水在容器内外壁全面清洗,经常擦洗锅体,保持外表清洁和内胆光亮,达到耐用的目的。

二、注意事项
 
  1.实验室反应釜是在常温下工作,必须正常通冷却水,以免磁钢磁性削减和退磁。
 
  2.加热设定和加热升速(100℃/h),不许过大升速。
 
First. the use and maintenance
 
  The use of laboratory reactor must be closed refrigerant inlet pipe valve, and put pot and clip refrigerant remaining in the sleeve, and then enter the material, start the blender, then open the steam valve and the electric power supply, to reach the required temperature, should first close the steam valve and the electric power supply, 2~3 minutes later, and then close the blender. After processing, the jacket and put the remaining condensed water, should rinse with warm water, brush off a sticky material, and then use the 40~500C base on the inner wall of the container clean, rinse with water, especially the no material (heat absorption medium) empty pot case, shall open the steam valve and the electric power supply. Pay special attention to the use of steam pressure shall not exceed the rated working pressure. Maintenance of laboratory reactor should always pay attention to the whole equipment and reducer work, lack of lubricants for deceleration should be added immediately, the electric heating medium oil every six months to be replaced on the jacket and cover and other parts of the safety valve, pressure gauge, thermometer, distillation hole, electric heating rods, electrical instrument should be regularly check, if there is failure to immediately replace or repair equipment when not in use, be sure to use warm water in the inner wall and the outer wall of the container comprehensive cleaning, regular cleaning of the pot body, keep clean and bright and durable liner, achieve the objective.
 
Second. matters needing attention
 
  1. laboratory reactor is working at normal temperature, must be normal cooling water, so as to avoid magnetic steel magnetic reduction and demagnetization.
 
  2. heating setting and heating up speed (100 /h), not too large lifting speed.

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